Although based on sophisticated science, the spectroscope itself is a simple device that needs only a few adjustments to use. All models have ways of adjusting the focus and the amount of light entering the instrument. Advanced models also have ways to adjust the focus and position of a scale for identifying light wavelengths. These general spectroscope instructions will help novice gemologists and hobbyists get familiar with the instrument’s basic operation.
What Is A Spectroscope?
The spectroscope is an important tool for identifying gemstones. Since gemstone species have characteristic structural and chemical properties, gems selectively absorb specific wavelengths of visible light. Gemologists use spectroscopes to view the absorption spectra of unknown gemstones and compare those patterns to those of known gemstone species.
For in-depth explanations of spectroscope operation and research techniques and advanced spectroscope instructions, read Don Clark’s article on the spectroscope.
Examine Your Spectroscope
Take your new spectroscope, point it towards a window or bright light, and look through the eyepiece. You should see a rectangular shaped rainbow spectrum, like the picture below. (Make sure you’re looking through the correct end).
If you have an advanced spectroscope, you should also see a scale. If it’s not immediately visible, try moving your head slightly to either side. Find the scale adjustment and turn it. You will see the scale move from side to side.
Find A Gemstone’s Absorption Lines
Place your spectroscope and a gem of known identity in the spectroscope’s stand. (If your model doesn’t have a stand, Don Clark’s spectroscope article offers some alternative techniques).
Next, adjust the amount of light entering the spectroscope. Slowly turn the light opening. Watch the spectrum through the eyepiece as you do this. As you adjust the light opening, the absorption lines (dark lines on the spectrum) will come into view. Try different settings until the absorption lines are most clearly visible.
If you can’t find the absorption lines, make sure the light is passing through the gem and into the end of your spectroscope. Turn off all other room lights so they’re not affecting your reading. Make sure you’re using a gem with a distinctive absorption pattern, like a natural or synthetic ruby.
If you’re still having trouble finding the absorption lines, you may not be looking straight down the tube. Set the light opening to the middle position and move your head slightly from side to side until you see the lines.
Focus Your Spectroscope
Once you find the absorption lines, focus the spectroscope. Depending on your model, you can do this by sliding a tube in and out or by turning a ring. You will notice that the absorption lines don’t become clear all at once. When one end of the spectrum is in focus, the other end will be slightly fuzzy. You may need to readjust the focus to see all the significant absorption lines.
Calibrate Your Spectroscope’s Scale
If you have an advanced spectroscope with a scale, focus your instrument until the scale is clear and easy to read.
Ruby displays strong double absorption lines at 475 and 476.5 and at 692.8 and 694.2 nanometers (nm). Choose a strong line, such as 475 nm. Adjust the scale position until the 475 marker lines up with the strong absorption line you are viewing. The scale markers at 476.5, 692.8, and 694.2 nm should then line up with the other strong absorption lines. Adjust the scale until the markers are on the known strong lines of the ruby absorption spectrum.
You’ve now properly calibrated your scale. However, you may need to make subtle adjustments to the scale when you view other stones. You can always use a gemstone with distinctive absorption lines to recalibrate your scale if it’s moved inadvertently.